3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester

Base Information

• Chemical Name: 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester
• CAS No.: 129871-71-2
• Molecular Formula: C₁₃H₁₄F₃NO₆S
• Molecular Weight: 369.318

Synonyms:3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester

Chemical Property of 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester

Chemical Property:

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Technology Process of 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester

There total 2 articles about 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

3-Hydroxy-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (91446-72-9) → 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (129871-71-2) + 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (129871-72-3)

Guidance literature:

With triethylamine; for 15h; Ambient temperature;

Reference yield: 20.0%

3-Hydroxy-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (91446-72-9) + methanesulfonyl chloride (124-63-0) → 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (129871-71-2) + 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (129871-72-3)

Guidance literature:

With triethylamine; for 15h; Ambient temperature;

Reference yield: 86.0%

trimethylsilyl bromide (2857-97-8) + 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester (129871-71-2) → 3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)(trimethylsilyl)amino>propansaeure-methylester (129871-73-4)

Guidance literature:

With triethylamine; In diethyl ether; for 5h; Ambient temperature;

upstream raw materials:

3-Hydroxy-3-phenyl-2-<(trifluoracetyl)amino>propansaeure-methylester

methanesulfonyl chloride

Downstream raw materials:

3-(Methylsulfonyloxy)-3-phenyl-2-<(trifluoracetyl)(trimethylsilyl)amino>propansaeure-methylester

3-Phenyl-2-<(trifluoracetyl)amino>-2-propensaeure-methylester

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