1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

Base Information

Chemical Name:1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester
CAS No.:1427019-02-0
Molecular Formula:C₄₄H₃₆Cl₂N₄O₄
Molecular Weight:755.7
Hs Code.:

Synonyms:1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

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Chemical Property of 1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

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Technology Process of 1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

There total 3 articles about 1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 629-03-8
1 ,6-dibromohexane

: 1427019-68-8
9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid

: 1427019-02-0
1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 6 - 10h;
DOI:10.1039/c4md00098f

Reference yield:

: 74214-62-3
ethyl 9H-pyrido[3,4-b]indole-3-carboxylate

: 1427019-02-0
1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C

1.2: 20 °C

2.1: sodium hydroxide / water; ethanol / 2 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C

With sodium hydride; potassium carbonate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 766-80-3
1-bromomethyl-3-chlorobenzene

: 1427019-02-0
1,6-bis[9-(3-chlorobenzyl)-β-carboline-3-carboxylic acid]hexanediyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C

1.2: 20 °C

2.1: sodium hydroxide / water; ethanol / 2 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C

With sodium hydride; potassium carbonate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;