benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

Base Information

Chemical Name:benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide
CAS No.:195516-38-2
Molecular Formula:C₂₂H₂₆F₆OSeSi
Molecular Weight:527.484
Hs Code.:

Synonyms:benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

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Technology Process of benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

There total 3 articles about benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 195516-37-1
2-(2-Benzylselanyl-phenyl)-1,1,1,3,3,3-hexafluoro-propan-2-ol

: 195516-38-2
benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

Guidance literature:: With triethylamine; In dichloromethane; 1.) 0 deg C, 2.) 40 deg C, 1 d;
DOI:10.1039/a704277i

Reference yield:

: 70091-67-7
lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide

: 195516-38-2
benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

2: 88 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 2.) 40 deg C, 1 d

With triethylamine; In dichloromethane;
DOI:10.1039/a704277i

Reference yield:

: 100-39-0
benzyl bromide

: 195516-38-2
benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

2: 88 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 2.) 40 deg C, 1 d

With triethylamine; In dichloromethane;
DOI:10.1039/a704277i