1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

Base Information

Chemical Name:1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester
CAS No.:117822-02-3
Molecular Formula:C₁₈H₂₃NO₅
Molecular Weight:333.384
Hs Code.:

Synonyms:1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

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Technology Process of 1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

There total 2 articles about 1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-37-8
1-(3-Methoxyphenyl)ethanone

: 117822-02-3
1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 65.4 percent / ammonium acetate, acetic acid / benzene / 20 h / Heating

2: 1.) hexamethyldisilazane, n-butyllithium / 1.) THF, hexane, 15 min, -78 deg C, 2.) 35 min, THF, 30 min, -78 deg C

With ammonium acetate; n-butyllithium; acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In benzene;

Reference yield:

: 80534-78-7
methyl-1 metamethoxybenzylidene cyanoacetate d'ethyle

: 141-78-6
ethyl acetate

: 117822-02-3
1-Cyano-2-(3-methoxyphenyl)-2-methyl-1,3-propandicarbonsaeurediethylester

Guidance literature:: With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1.) THF, hexane, 15 min, -78 deg C, 2.) 35 min, THF, 30 min, -78 deg C;