5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

Base Information

Chemical Name:5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate
CAS No.:1402161-28-7
Molecular Formula:C₄H₆O₆*C₂₂H₂₅N₃O₂
Molecular Weight:513.547
Hs Code.:

Synonyms:5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

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Chemical Property of 5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

Chemical Property:

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Technology Process of 5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

There total 5 articles about 5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-69-4,138508-61-9
L-Tartaric acid

: 1338365-54-0,1201180-97-3
5-(2-aminopropyl)-1-[3-(benzoyloxy)propyl]-2,3-dihydro-7-cyano-1H-indole

: 1402161-28-7
5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

Guidance literature:: L-Tartaric acid; 5-(2-aminopropyl)-1-[3-(benzoyloxy)propyl]-2,3-dihydro-7-cyano-1H-indole; In isopropyl alcohol; at 20 - 50 ℃; for 5h;

With palladium/alumina; hydrogen; at 100 ℃; for 24h; under 380.026 Torr; Temperature; Solvent; Reagent/catalyst; Pressure;

Reference yield:

: C₂₉H₃₄N₂O₃

: 1402161-28-7
5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 1 h / 30 °C

2.1: trichlorophosphate

3.1: hydroxylamine hydrochloride; pyridine

4.1: acetic anhydride

5.1: palladium on activated charcoal; hydrogen

5.2: Inert atmosphere

With pyridine; palladium on activated charcoal; hydroxylamine hydrochloride; hydrogen; acetic anhydride; trichlorophosphate; In toluene;

Reference yield:

: C₃₇H₄₀N₂O₅

: 1402161-28-7
5-[2-aminopropyl]-2,3-dihydro-1-[3-(benzoyloxy)propyl]-1H-indole-7-carbonitrile L-(+)-tartrate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate

2.1: hydroxylamine hydrochloride; pyridine

3.1: acetic anhydride

4.1: palladium on activated charcoal; hydrogen

4.2: Inert atmosphere

With pyridine; palladium on activated charcoal; hydroxylamine hydrochloride; hydrogen; acetic anhydride; trichlorophosphate;