C₇₁H₇₁Cl₂N₁₁O₁₁

Base Information

Chemical Name:C₇₁H₇₁Cl₂N₁₁O₁₁
CAS No.:439599-73-2
Molecular Formula:C₇₁H₇₁Cl₂N₁₁O₁₁
Molecular Weight:1325.32
Hs Code.:

C<sub>71</sub>H<sub>71</sub>Cl<sub>2</sub>N<sub>11</sub>O<sub>11</sub>

Synonyms:C₇₁H₇₁Cl₂N₁₁O₁₁

Suppliers and Price of C₇₁H₇₁Cl₂N₁₁O₁₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇₁H₇₁Cl₂N₁₁O₁₁

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₇₁H₇₁Cl₂N₁₁O₁₁

There total 7 articles about C₇₁H₇₁Cl₂N₁₁O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: N-[3-(2-aminoacetyl)-5-benzyloxy-1-chloromethyl-2,3-dihydro-1H-benzo[e]indol-7-yl]acetamide hydrochloride

: 439599-64-1
5-benzyloxy-7-(3-{5-[5-(5-carboxy-1-methyl-1H-pyrrol-3-ylcarbamoyl)-1-methyl-1H-pyrrol-3-ylcarbamoyl]-1-methyl-1H-pyrrol-3-ylcarbamoyl}propionylamino)-1-chloromethyl-1,2-dihydrobenzo[e]indole-3-carboxylic acid tert-butyl ester

: 439599-73-2
C₇₁H₇₁Cl₂N₁₁O₁₁

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1039/b303650m

Reference yield:

: 286374-31-0
7-amino-5-benzyloxy-1-chloromethyl-1,2-dihydrobenzo[e]indole-3-carboxylic acid tert-butyl ester

: 439599-73-2
C₇₁H₇₁Cl₂N₁₁O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1: DIEA

2: HCl / dioxane / 5 h / 23 °C

3: 1.05 g / HOBt; EDCI; NaHCO₃ / dimethylformamide / 12 h / 20 °C

4: HCl / dioxane / 5 h / 23 °C

5: 72 percent / HOBt; EDCI; NaHCO₃ / dimethylformamide / 12 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b303650m

Reference yield:

: 69910-21-0
1-methyl-4-({1-methyl-4-[(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)amino]-1H-pyrrole-2-carbonyl}amino)-1H-pyrrole-2-carboxylic acid methyl ester

: 439599-73-2
C₇₁H₇₁Cl₂N₁₁O₁₁

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / methanol / 2 h / 2585.81 Torr

2: 1.40 g / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

3: 81 percent / NaOH / methanol / 20 °C

4: 72 percent / HOBt; EDCI; NaHCO₃ / dimethylformamide / 12 h / 20 °C

With sodium hydroxide; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/b303650m