2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

Base Information

Chemical Name:2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane
CAS No.:161690-36-4
Molecular Formula:C₇₂H₁₄₀Ge₂S₂Si₁₂
Molecular Weight:1552.24
Hs Code.:

Synonyms:2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

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Chemical Property of 2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

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Technology Process of 2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

There total 3 articles about 2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 135139-69-4
5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane

: 1608-26-0
Hexamethylphosphorous triamide

: 161690-36-4
2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

Guidance literature:: In tetrahydrofuran; freezing, heating (90 .degrre.C, 1 day);
DOI:10.1021/ja991147x

Reference yield: 57.0%

: 680-31-9
N,N,N,N,N,N-hexamethylphosphoric triamide

: 135139-69-4
5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane

: 161690-36-4
2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

: 135139-74-1
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

Guidance literature:: With water; In tetrahydrofuran; treatment of Ge-compd with 3 equiv. of HMPT in THF at -78°C;

Reference yield: 49.0%

: 135139-69-4
5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane

: 1608-26-0
Hexamethylphosphorous triamide

: 161690-36-4
2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane

: 135139-74-1
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

Guidance literature:: In tetrahydrofuran; -78°C, warming (room temp., 10 h); chromatography (SiO2, hexane/CH2Cl2 (10:1)); elem. anal.;
DOI:10.1021/ja991147x