[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

Base Information

• Chemical Name: [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane
• CAS No.: 135139-74-1
• Molecular Formula: C₃₆H₇₂GeOSSi₆
• Molecular Weight: 794.136

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

Chemical Property:

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane

There total 10 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane (135139-69-4) → 2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane (161690-36-4) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane (135139-74-1)

Guidance literature:

With water; In tetrahydrofuran; treatment of Ge-compd with 3 equiv. of HMPT in THF at -78°C;

Reference yield: 49.0%

5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane (135139-69-4) + Hexamethylphosphorous triamide (1608-26-0) → 2,4-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2,4-dimesityl-1,2,3,4-dithiagermetane (161690-36-4) + [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane (135139-74-1)

Guidance literature:

In tetrahydrofuran; -78°C, warming (room temp., 10 h); chromatography (SiO2, hexane/CH2Cl2 (10:1)); elem. anal.;

DOI:10.1021/ja991147x

Reference yield: 35.0%

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane (135139-69-4) → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](hyroxy)(mercapto)(mesityl)germane (135139-74-1) + cis-(GeS(C6H2(CH(Si(CH3)3)2)3)(C6H2(CH3)3))2 (135139-75-2)

Guidance literature:

In tetrahydrofuran; -78°C;

upstream raw materials:

N,N,N,N,N,N-hexamethylphosphoric triamide

5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-mesityl-1,2,3,4,5-tetrathiagermolane

Hexamethylphosphorous triamide

GeS₄(C(C₆H₅)2)(C₆H₂(CH(Si(CH₃)3)2)3)(C₆H₂(CH₃)3)

Downstream raw materials:

(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)hydroxy(mesityl)(methylthio)germane

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