4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid

Base Information

• Chemical Name: 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid
• CAS No.: 948990-79-2
• Molecular Formula: C₂₀H₂₁BN₂O₅
• Molecular Weight: 380.208

Synonyms:4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid

Chemical Property of 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid

Chemical Property:

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Technology Process of 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid

There total 1 articles about 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-((R)-4-benzoyl-2-methylpiperazin-1-yl)-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethane-1,2-dione (948990-78-1) → 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid (948990-79-2)

Guidance literature:

With sodium periodate; ammonium acetate; In water; acetone; at 25 ℃; for 24h;

DOI:10.1021/jm900330x

Reference yield: 56.0%

pyrrolidine (123-75-1) + 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid (948990-79-2) → 1-((R)-4-benzoyl-2-methylpiperazin-1-yl)-2-(4-pyrrolidin-1-ylphenyl)ethane-1,2-dione

Guidance literature:

With copper diacetate; triethylamine; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/jm900330x

Reference yield: 36.0%

dimethylenecyclourethane (497-25-6) + 4-[2-(4-benzoyl-2(R)-methylpiperazin-1-yl)-2-oxoacetyl]phenylboronic acid (948990-79-2) → 1-((R)-4-benzoyl-2-methylpiperazin-1-yl)-2-[4-(2-oxooxazolidin-3-yl)phenyl]ethane-1,2-dione

Guidance literature:

With copper diacetate; triethylamine; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/jm900330x

upstream raw materials:

1-((R)-4-benzoyl-2-methylpiperazin-1-yl)-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethane-1,2-dione

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