(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

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Chemical Name:(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid
CAS No.:79336-04-2
Molecular Formula:C₂₀H₂₇N₃O₉
Molecular Weight:453.449
Hs Code.:

Synonyms:(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

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Chemical Property of (2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

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Technology Process of (2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

There total 6 articles about (2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79336-02-0
(2S,6R)-6-Amino-2-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-6-hydrazinocarbonyl-hexanoic acid

: 79336-04-2
(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

Guidance literature:: With sodium periodate; sulfuric acid; In water; at 0 ℃;
DOI:10.1021/jm00346a001

Reference yield:

: 80226-11-5
(2S,6R)-2-Amino-6-tert-butoxycarbonylamino-7-(N'-tert-butoxycarbonyl-hydrazino)-7-oxo-heptanoic acid

: 79336-04-2
(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran; dimethylformamide / Ambient temperature

2: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) CH₂Cl₂, from -15 to -10 deg C, 2.) from -10 to 0 deg C

3: 1 N aq. NaOH / methanol

4: trifluoroacetic acid / Ambient temperature

5: NaIO₄, 0.1 N H₂SO₄ / H₂O / 0 °C

With 4-methyl-morpholine; sodium hydroxide; sodium periodate; sulfuric acid; trifluoroacetic acid; isobutyl chloroformate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00346a001

Reference yield:

: 94271-26-8
C₂₀H₄₀N₄O₇Si

: 79336-04-2
(2S,6R)-2-Amino-6-((R)-4-benzyloxycarbonylamino-4-carboxy-butyrylamino)-heptanedioic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) CH₂Cl₂, from -15 to -10 deg C, 2.) from -10 to 0 deg C

2: 1 N aq. NaOH / methanol

3: trifluoroacetic acid / Ambient temperature

4: NaIO₄, 0.1 N H₂SO₄ / H₂O / 0 °C

With 4-methyl-morpholine; sodium hydroxide; sodium periodate; sulfuric acid; trifluoroacetic acid; isobutyl chloroformate; In methanol; water;
DOI:10.1021/jm00346a001