1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

Base Information

Chemical Name:1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)
CAS No.:1349064-27-2
Molecular Formula:C₃₀H₃₀Cl₂N₆S₄
Molecular Weight:673.778
Hs Code.:

Synonyms:1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

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Chemical Property of 1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

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Technology Process of 1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

There total 8 articles about 1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 5,5’-disulfanediylbis(2-chloroaniline) dihydrochloride

: 222734-73-8
N-methyl-N-(3-(methylthio)phenyl)cyanamide

: 1349064-27-2
1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

Guidance literature:: at 140 - 145 ℃; for 5h;
DOI:10.1002/jlcr.3831

Reference yield:

: ClH*C₁₂H₁₀Cl₂N₂S₂

: 222734-73-8
N-methyl-N-(3-(methylthio)phenyl)cyanamide

: 1349064-27-2
1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

Guidance literature:: at 130 ℃; for 36h; Sealed tube; Inert atmosphere;

Reference yield:

: 97-08-5
3-nitro-4-chlorosulfonyl chloride

: 1349064-27-2
1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; tin(ll) chloride / water / 3 h / 125 °C

2: iodine / water

3: 17 h / 130 °C

With hydrogenchloride; iodine; tin(ll) chloride; In water;