C₁₄H₃₀O₂Si

Base Information

Chemical Name:C₁₄H₃₀O₂Si
CAS No.:1422463-26-0
Molecular Formula:C₁₄H₃₀O₂Si
Molecular Weight:258.476
Hs Code.:

C<sub>14</sub>H<sub>30</sub>O<sub>2</sub>Si

Synonyms:C₁₄H₃₀O₂Si

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Chemical Property of C₁₄H₃₀O₂Si

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Technology Process of C₁₄H₃₀O₂Si

There total 4 articles about C₁₄H₃₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422463-28-2
C₂₂H₃₈O₃Si

: 1422463-26-0
C₁₄H₃₀O₂Si

: 123-11-5
4-methoxy-benzaldehyde

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h; pH=7; Overall yield = 97 %; Overall yield = 3.9 g;
DOI:10.1021/jo3026077

Reference yield:

: C₂₆H₃₇NO₅S

: 1422463-26-0
C₁₄H₃₀O₂Si

: 123-11-5
4-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C / Inert atmosphere

3: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C / pH 7

With 1H-imidazole; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo3026077

Reference yield:

: 1422463-22-6
C₁₆H₂₂O₃

: 1422463-26-0
C₁₄H₃₀O₂Si

: 123-11-5
4-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C / pH 7

With 1H-imidazole; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo3026077