cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester

Base Information

• Chemical Name: cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester
• CAS No.: 1082204-94-1
• Molecular Formula: C₂₁H₂₂O₁₄
• Molecular Weight: 498.397

Synonyms:cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester

Chemical Property of cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester

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Technology Process of cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester

There total 1 articles about cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

methanol (67-56-1) + 7-bromo-1,2,3,4,5,6,7-hepta(methoxycarbonyl)cyclohepta-1,3,5-triene → hexamethyl benzenehexacarboxylate (6237-59-8) + cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester (1082204-94-1) + 7-methoxy-1,2,3,4,5,6,7-hepta(methoxycarbonyl)cyclohepta-1,3,5-triene

Guidance literature:

In methanol; at 60 ℃; for 20h; Reagent/catalyst; Time; Inert atmosphere;

DOI:10.1007/s11172-015-0851-4

Reference yield: 95.0%

cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester (1082204-94-1) + benzylamine (100-46-9) → heptamethyl 8-benzyl-8-azabicyclo[3.2.1]oct-2-ene-1,2,3,4,5,6,7-heptacarboxylate

Guidance literature:

In chloroform; at 20 ℃; for 24h; regioselective reaction;

DOI:10.1016/j.tetlet.2009.07.114

Reference yield: 50.0%

cycloheptatriene-1,2,3,4,5,6,7-heptacaarboxylic acid heptamethyl ester (1082204-94-1) + phenethylamine (64-04-0) → C28H29NO13 (1191924-55-6) + C28H29NO13 + C29H33NO14

Guidance literature:

In para-xylene; at 20 ℃; for 24h; optical yield given as %de; stereoselective reaction;

DOI:10.1016/j.tetlet.2009.07.114

upstream raw materials:

methanol

Downstream raw materials:

C₂₈H₂₉NO₁₃

1-benzyl-3-[(1,2,3-trimethoxycarbonyl)prop-1-enyl]-4,5,6-trimethoxycarbonylpyridin-2-one

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