(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

Base Information

Chemical Name:(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester
CAS No.:157896-17-8
Molecular Formula:C₅₈H₆₁N₉O₁₃
Molecular Weight:1092.17
Hs Code.:

(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

Synonyms:(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

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Chemical Property of (S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

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Technology Process of (S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

There total 3 articles about (S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: N-(L-γ-glutamyl)-L-glutamic acid tribenzyl ester hydrochloride

: 157896-14-5
(S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester

: 157896-17-8
(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 157896-17-8
(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / Cs₂CO₃ / dimethylsulfoxide

2: 87 percent / Et₃N, diphenylphosphoride azide / dimethylformamide

With diphenyl phosphoryl azide; caesium carbonate; triethylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: <6(S)-5-formyl-5,6,7,8-tetrahydropteroyl>-mono-L-glutamic acid

: 157896-17-8
(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / Cs₂CO₃ / dimethylsulfoxide

2: 87 percent / Et₃N, diphenylphosphoride azide / dimethylformamide

With diphenyl phosphoryl azide; caesium carbonate; triethylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide;