(S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester

Base Information

• Chemical Name: (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester
• CAS No.: 157896-14-5
• Molecular Formula: C₂₇H₂₉N₇O₇
• Molecular Weight: 563.57

Synonyms:(S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester

Chemical Property of (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester

Chemical Property:

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Technology Process of (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester

There total 1 articles about (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

benzyl bromide (100-39-0) + <6(S)-5-formyl-5,6,7,8-tetrahydropteroyl>-mono-L-glutamic acid → (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester (157896-14-5)

Guidance literature:

With caesium carbonate; In dimethyl sulfoxide;

Reference yield: 99.0%

(S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester (157896-14-5) + (S)-2-{(S)-4-[(S)-4-((S)-4-Amino-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-4-benzyloxycarbonyl-butyrylamino}-pentanedioic acid dibenzyl ester; hydrochloride → C82H87N11O19

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide;

Reference yield: 89.0%

N--L-glutamic acid tetrabenzyl ester hydrochloride (83816-93-7) + (S)-2-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-pentanedioic acid 1-benzyl ester (157896-14-5) → C70H74N10O16 (157896-16-7)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide;

upstream raw materials:

benzyl bromide

Downstream raw materials:

(S)-2-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-pentanedioic acid dibenzyl ester

(S)-2-[(S)-4-((S)-4-{4-[((5R,6S)-2-Amino-5-formyl-4-oxo-3,4,5,6,7,8-hexahydro-pteridin-6-ylmethyl)-amino]-benzoylamino}-4-benzyloxycarbonyl-butyrylamino)-4-benzyloxycarbonyl-butyrylamino]-pentanedioic acid dibenzyl ester

C₇₀H₇₄N₁₀O₁₆

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