2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

Base Information

Chemical Name:2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate
CAS No.:1213790-39-6
Molecular Formula:C₂₁H₂₂BrN₃O₅
Molecular Weight:476.327
Hs Code.:

Synonyms:2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

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Chemical Property of 2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

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Technology Process of 2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

There total 5 articles about 2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1213790-38-5
tert-butyl 4-bromo-3-(bromomethyl)phenyl(5-cyano-6-methoxypyridin-2-yl)carbamate

: 127-09-3
sodium acetate

: 1213790-39-6
2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

Guidance literature:: In N,N-dimethyl-formamide; at 50 ℃; for 2h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1213790-39-6
2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / N,N-dimethyl-formamide / 72 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere; Cooling with ice

2.2: 50 °C / Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 2 h / 95 °C / Inert atmosphere

4.1: N,N-dimethyl-formamide / 2 h / 50 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; triethylamine; In tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

: 6933-10-4
amino-5-bromo-2-toluene

: 1213790-39-6
2-bromo-5-(tert-butoxycarbonyl(5-cyano-6-methoxypyridin-2-yl)amino)benzyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / N,N-dimethyl-formamide / 72 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere; Cooling with ice

2.2: 50 °C / Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 2 h / 95 °C / Inert atmosphere

4.1: N,N-dimethyl-formamide / 2 h / 50 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; triethylamine; In tetrachloromethane; N,N-dimethyl-formamide;