acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

Base Information

Chemical Name:acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride
CAS No.:1073186-93-2
Molecular Formula:C₂₃H₃₇NO₃S*ClH
Molecular Weight:444.079
Hs Code.:

Synonyms:acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

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Chemical Property of acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

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Technology Process of acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

There total 5 articles about acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1073186-92-1
4-(2-acetoxy-ethyl)-4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidine-1-carboxylic acid tert-butyl ester

: 1073186-93-2
acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 3h;

Reference yield:

tert-butyl 4-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate: 135716-08-4
tert-butyl 4-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate

: 1073186-93-2
acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine / 15 h / 90 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h

3: dmap; triethylamine / dichloromethane / 3 h

4: hydrogenchloride / 1,4-dioxane / 3 h

With piperidine; hydrogenchloride; dmap; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: C₂₆H₄₃NO₄S

: 1073186-93-2
acetic acid 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidin-4-yl]-ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 3 h

2: hydrogenchloride / 1,4-dioxane / 3 h

With hydrogenchloride; dmap; triethylamine; In 1,4-dioxane; dichloromethane;