(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

Base Information

Chemical Name:(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine
CAS No.:1448530-83-3
Molecular Formula:C₂₃H₄₄BrNO₃Si₂
Molecular Weight:518.682
Hs Code.:

Synonyms:(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

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Chemical Property of (S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

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Technology Process of (S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

There total 3 articles about (S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₅₈BrNO₃Si₃

: 1448530-83-3
(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

Guidance literature:: With ammonium chloride; In dichloromethane; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.009

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1448530-83-3
(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: ammonium chloride / water; dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; ammonium chloride; triethylamine; In dichloromethane; water;
DOI:10.1016/j.tet.2013.05.009

Reference yield:

: 1177255-31-0
bromotyrosinol

: 1448530-83-3
(S)-1-(2-bromo-5-((tert-butyldimethylsilyl)oxy)-4-methoxy-3-methylphenyl)-3-((tert-butyldimethylsilyl)oxy)propan-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: ammonium chloride / water; dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; ammonium chloride; triethylamine; In dichloromethane; water;
DOI:10.1016/j.tet.2013.05.009