1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate
CAS No.:959778-67-7
Molecular Formula:C₁₄H₁₉N₃O₆
Molecular Weight:325.321
Hs Code.:

Synonyms:1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

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Chemical Property of 1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

Chemical Property:

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Technology Process of 1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

There total 3 articles about 1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 2486-66-0
2-ethoxy-4-nitrobenzoic acid

: 959778-67-7
1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

: 619-19-2
2-hydroxy-4-nitrobenzoic acid

: 959778-67-7
1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydroxide; ethanol; water / 20 °C

2.2: Acidic conditions

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With sodium hydroxide; ethanol; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 910572-96-2
2-ethoxy-4-nitro-benzoic acid ethyl ester

: 959778-67-7
1,1-dimethylethyl 2-{[2-(ethyloxy)-4-nitrophenyl]carbonyl}hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; ethanol; water / 20 °C

1.2: Acidic conditions

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With sodium hydroxide; ethanol; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;