(E)-2-Phenyl-ethenesulfonic acid benzoylamide

Base Information

Chemical Name:(E)-2-Phenyl-ethenesulfonic acid benzoylamide
CAS No.:134641-05-7
Molecular Formula:C₁₅H₁₃NO₃S
Molecular Weight:287.339
Hs Code.:

Synonyms:(E)-2-Phenyl-ethenesulfonic acid benzoylamide

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Chemical Property of (E)-2-Phenyl-ethenesulfonic acid benzoylamide

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Technology Process of (E)-2-Phenyl-ethenesulfonic acid benzoylamide

There total 3 articles about (E)-2-Phenyl-ethenesulfonic acid benzoylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 108-86-1,52753-63-6
bromobenzene

: 134640-90-7
(2-(benzoylsulfamoyl)ethyl)pyridinium chloride

: 134641-05-7
(E)-2-Phenyl-ethenesulfonic acid benzoylamide

Guidance literature:: With triethylamine; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 140 ℃;
DOI:10.1246/bcsj.64.1431

Reference yield: 19.0%

: 64984-09-4
(E)-(2-phenylethenyl)sulfonamide

: 98-88-4
benzoyl chloride

: 134641-05-7
(E)-2-Phenyl-ethenesulfonic acid benzoylamide

Guidance literature:: With triethylamine; In acetone; Ambient temperature;
DOI:10.1246/bcsj.64.1431

Reference yield:

: 591-50-4
iodobenzene

: 134641-05-7
(E)-2-Phenyl-ethenesulfonic acid benzoylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / palladium acetate, triphenylphosphine / dimethylformamide / 24 h / 140 °C

2: 19 percent / triethylamine / acetone / Ambient temperature

With triethylamine; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.64.1431