phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside
CAS No.:1309374-71-7
Molecular Formula:C₆₀H₅₀O₁₅S
Molecular Weight:1043.11
Hs Code.:

Synonyms:phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

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Chemical Property of phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

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Technology Process of phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

There total 4 articles about phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1309374-70-6
phenyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1-thio-α-L-rhamnopyranoside

: 98-88-4
benzoyl chloride

: 1309374-71-7
phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: With pyridine; for 4h;
DOI:10.1016/j.steroids.2011.02.010

Reference yield:

: 149707-76-6
O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl) trichloroacetimidate

: 1309374-71-7
phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.17 h / -20 °C / Molecular sieve

1.2: -20 °C

2.1: acetic acid / 5 h / 80 °C

3.1: pyridine / 4 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; acetic acid; In dichloromethane;
DOI:10.1016/j.steroids.2011.02.010

Reference yield:

: 131087-35-9
phenyl 2,3-O-isopropylidene-1-thio-α-L-rhamnopyranoside

: 1309374-71-7
phenyl 2,3-di-O-benzoyl-4-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glycopyranosyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.17 h / -20 °C / Molecular sieve

1.2: -20 °C

2.1: acetic acid / 5 h / 80 °C

3.1: pyridine / 4 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; acetic acid; In dichloromethane;
DOI:10.1016/j.steroids.2011.02.010