{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

Base Information

Chemical Name:{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester
CAS No.:183273-10-1
Molecular Formula:C₃₃H₂₈BrNO₆
Molecular Weight:614.492
Hs Code.:

Synonyms:{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

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Chemical Property of {4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

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Technology Process of {4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

There total 1 articles about {4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1026914-86-2
[4-(3-Amino-4-bromo-phenoxymethyl)-phenoxy]-acetic acid allyl ester

: 183273-10-1
{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

Guidance literature:: With pyridine; In dichloromethane; at 22 ℃; for 1h;
DOI:10.1016/0040-4039(96)01635-8

Reference yield: 71.0%

: 183273-10-1
{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

: {4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid

Guidance literature:: With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 22 ℃; for 0.666667h;
DOI:10.1016/0040-4039(96)01635-8

Reference yield:

: 183273-10-1
{4-[4-Bromo-3-(9H-fluoren-9-ylmethoxycarbonylamino)-phenoxymethyl]-phenoxy}-acetic acid allyl ester

: 1-(3-Benzyl-6-hydroxy-indol-1-yl)-propan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Bu₃SnH / Pd(Ph₃P)4 / CH₂Cl₂ / 0.67 h / 22 °C

With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane;
DOI:10.1016/0040-4039(96)01635-8