N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide

Base Information

• Chemical Name: N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide
• CAS No.: 71332-56-4
• Molecular Formula: C₁₂H₁₄N₂O
• Molecular Weight: 202.256
• Mol file: 71332-56-4.mol

Synonyms:N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide

Chemical Property of N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide

There total 3 articles about N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

1-benzoyl-2,2-dimethyl-2-(2-propyn-1-yl)-2-hydrazinium bromide → N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide (71332-56-4)

Guidance literature:

With sodium hydroxide; In water; at 20 ℃; for 2h;

DOI:10.1023/A:1025644620981

Reference yield:

benzoyl chloride (98-88-4) → N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide (71332-56-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 21 percent / benzene / 20 °C

2: 59 percent / methanol / 6 h / 50 °C

3: 51 percent / NaOH / H₂O / 2 h / 20 °C

With sodium hydroxide; In methanol; water; benzene;

DOI:10.1023/A:1025644620981

Reference yield:

→ N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide (71332-56-4)

Guidance literature:

Hydrazinium 1, Na-Carbonat;

upstream raw materials:

benzoyl chloride

Downstream raw materials:

6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide