6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

Base Information

Chemical Name:6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide
CAS No.:72072-17-4
Molecular Formula:Br*C₁₂H₁₄BrN₂O
Molecular Weight:362.064
Hs Code.:

Synonyms:6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

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Technology Process of 6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

There total 3 articles about 6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 627-16-7
1,3-dibromoprop-1-yne

: 1128-86-5
1-benzoyl-2,2-dimethylhydrazine

: 72072-17-4
6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

Guidance literature:: In methanol; at 50 ℃; for 5h;
DOI:10.1023/A:1015028806581 DOI:10.1007/s11176-005-0246-6

Reference yield:

: 71332-56-4
N-[dimethyl(2-propyn-1-yl)ammonio]benzoylimide

: 72072-17-4
6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

Guidance literature:: With bromine; In chloroform;

Reference yield:

: 98-88-4
benzoyl chloride

: 72072-17-4
6-bromomethylidene-4,4-dimethyl-2-phenyl-5H-1,3,4-oxadiazinium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / benzene / 20 °C

2: 73 percent / methanol / 4 h / 50 °C

In methanol; benzene;
DOI:10.1023/B:RUJO.0000013127.32367.38