tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

Base Information

Chemical Name:tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate
CAS No.:1169930-14-6
Molecular Formula:C₁₈H₂₉NO₄
Molecular Weight:323.433
Hs Code.:

Synonyms:tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

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Chemical Property of tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

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Technology Process of tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

There total 1 articles about tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1169930-13-5
[3-(3-bromopropoxy)phenyl]methanol

: 143707-72-6
tert-butyl N-methyl-β-alaninate

: 1169930-14-6
tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;

Reference yield: 94.0%

: 1169930-14-6
tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

: 74-89-5
methylamine

: 1169930-15-7
Tert-butyl 3-(methyl(3-(3-((methylamino)methyl)phenoxy)-propyl)-amino)propanoate

Guidance literature:: tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate; With methanesulfonyl chloride; triethylamine; In dichloromethane; at -78 ℃; for 1.5h; Inert atmosphere;

methylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

Reference yield: 60.0%

: 1169930-14-6
tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate

: dichloro-N,N-bis-(2-chloroethyl)phosphoramide

: 1170861-53-6
C₂₂H₃₈Cl₂N₃O₅P

Guidance literature:: tert-butyl 3-((3-(3-(hydroxymethyl)-phenoxy)propyl)(methyl)amino)propanoate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 0.333333h; Inert atmosphere;

dichloro-N,N-bis-(2-chloroethyl)phosphoramide; In tetrahydrofuran; at -78 - 20 ℃; for 4h;

With ammonia; In tetrahydrofuran; dichloromethane; at -50 - 20 ℃; for 2h;