(6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1)

Base Information

Chemical Name:(6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1)
CAS No.:16456-97-6
Molecular Formula:C₂₂H₂₈N₂O₂Zn
Molecular Weight:417.867
Hs Code.:

Synonyms:Zinc,bis[2-[(butylimino)methyl]phenolato-N,O]-, (T-4)-; Zinc,bis[o-(N-butylformimidoyl)phenolato]- (6CI,7CI,8CI); Phenol,2-[(butylimino)methyl]-, zinc complex; Bis(N-butylsalicylaldiminato)zinc;Bis(N-butylsalicylideneaminato)zinc; NSC 253608

Suppliers and Price of (6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1)

Chemical Property:

Vapor Pressure:0.00113mmHg at 25°C
Boiling Point:300.3°C at 760 mmHg
Flash Point:121.2°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1)

There total 3 articles about (6Z)-6-[(butylamino)methylidene]cyclohexa-2,4-dien-1-one - zinc (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2565-54-0
N-salicylidene-butylamine

: 5970-45-6
zinc(II) acetate dihydrate

: 16456-97-6
[zinc(II)bis(N-butylsalicylideneiminate)]

Guidance literature:: In ethanol; addn. of solid Zn(AcO)2*2H2O to ligand soln.; stirring at elevated temp. up to complete dissoln., 2h; cooling; pptn.; recrystn. (EtOH); elem. anal.;

Reference yield:

: 2565-54-0
N-salicylidene-butylamine

: 7440-66-6
zinc

: 16456-97-6
[zinc(II)bis(N-butylsalicylideneiminate)]

Guidance literature:: In methanol; Electrochem. Process; Zn anode; working soln.: C11H15NO in MeOH, Et4NClO4 as a conducting additive, at current strength of 40 mA, voltage of 15 V for 1 h at room temp.; ppt. filtered off; recrystd. from EtOH, dried in vac. desiccator; elem. anal.;
DOI:10.1134/S1070328409020067

Reference yield:

: zinc(II) acetate hydrate

: 2565-54-0
N-salicylidene-butylamine

: 16456-97-6
[zinc(II)bis(N-butylsalicylideneiminate)]

Guidance literature:: In ethanol; EtOH soln. of Zn salt added to EtOH soln. of C11H15NO (molar ratio of 1:2), mixt. refluxed for 2 h; on cooling EtOH soln. of CH3ONa added; ppt. filtered off; recrystd. from EtOH; elem. anal.;
DOI:10.1134/S1070328409020067