[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

Base Information

Chemical Name:[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-
CAS No.:184291-86-9
Molecular Formula:C₇₉H₁₃₄N₂O₁₁SSi₃
Molecular Weight:1404.26
Hs Code.:

[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

Synonyms:[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

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Chemical Property of [2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

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Technology Process of [2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

There total 1 articles about [2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 184292-16-8
(6-aminohexyl)carbamic acid allyl ester

: C₇₃H₁₁₉NO₁₂SSi₃

: 184291-86-9
[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

Guidance literature:: With dmap; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/ja961374o

Reference yield:

: 184291-86-9
[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

: 184292-46-4
C₇₃H₁₃₀N₂O₁₂Si₃

Guidance literature:: With pH 7 buffer; mercury dichloride; In tetrahydrofuran; acetonitrile; for 0.333333h;
DOI:10.1021/ja961374o

Reference yield:

: 184291-86-9
[2S-(2β(3Z,5S,6S,7R,9S,11Z,13S,14S,15S,16Z,18S),3β,4β,5α,6α)]-14,18-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-19-{4-[(1,1-dimethylethyl)dimethylsilyl]oxy}tetrahydro-3,5-dimethyl-6-(phenylthio)-2H-pyran-2-yl-6-[(4-methoxyphenyl)methoxy]-9-

: 184291-87-0
[3S-(3α,4β,5β,6α(2S,3Z,5S,6S,7S,8Z,11S,13R,14S,15S,16Z))]-6-[2,6-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-14-[(4-methoxyphenyl)methoxy]-9-({[({5-[(2-propenyloxy)carbonyl]hexyl}amino)carbonyl]oxy}pentyl)-5,7,11,13,15-pentamethyl-12-oxo-3,8,16,18-n]

Guidance literature:: Multi-step reaction with 2 steps

1: 33 mg / HgCl₂, pH 7 buffer / tetrahydrofuran; acetonitrile / 0.33 h

2: Jones reagent / acetone / 0.5 h / 0 °C

With jones reagent; pH 7 buffer; mercury dichloride; In tetrahydrofuran; acetone; acetonitrile;
DOI:10.1021/ja961374o