1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

Base Information

Chemical Name:1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane
CAS No.:1601478-60-7
Molecular Formula:C₂₈H₄₂O₄Si₂
Molecular Weight:498.81
Hs Code.:

Synonyms:1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

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Chemical Property of 1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

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Technology Process of 1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

There total 1 articles about 1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 17100-66-2
2-(tetrahydropyranyloxy)methylbromobenzene

: 4342-61-4
1,2-dichlorotetramethylsilane

: 1601478-60-7
1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

Guidance literature:: 2-(tetrahydropyranyloxy)methylbromobenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 3.5h; Inert atmosphere;

1,2-dichlorotetramethylsilane; In diethyl ether; hexane; at 20 ℃; Inert atmosphere;
DOI:10.1246/cl.130919

Reference yield: 90.0%

: 1601478-60-7
1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

: 1601478-57-2
1,2-bis{2-(hydroxymethyl)phenyl}-1,1,2,2-tetramethyldisilane

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1246/cl.130919

Reference yield: 75.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1601478-60-7
1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

: 1601478-70-9
4-methoxyphenyl-(2-tetrahydropyranyloxy)methylphenyl-dimethylsilane

Guidance literature:: With copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); water; potassium carbonate; ruphos; In 1,4-dioxane; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1246/cl.130919