1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Base Information

Chemical Name:1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane
CAS No.:1601478-68-5
Molecular Formula:C₅₀H₆₂O₂Si₄
Molecular Weight:807.383
Hs Code.:

Synonyms:1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Suppliers and Price of 1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

There total 3 articles about 1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1601478-57-2
1,2-bis{2-(hydroxymethyl)phenyl}-1,1,2,2-tetramethyldisilane

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1601478-68-5
1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1246/cl.130919

Reference yield:

: 17100-66-2
2-(tetrahydropyranyloxy)methylbromobenzene

: 1601478-68-5
1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 3.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; toluene-4-sulfonic acid; In methanol; diethyl ether; hexane; N,N-dimethyl-formamide;
DOI:10.1246/cl.130919

Reference yield:

: 1601478-60-7
1,2-bis[2-{(2-tetrahydropyranyloxy)methyl}phenyl]-1,1,2,2-tetramethyldisilane

: 1601478-68-5
1,2-bis(2-{[(tert-butyldiphenylsilyl)oxy]methyl}phenyl)-1,1,2,2-tetramethyldisilane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

With 1H-imidazole; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1246/cl.130919