2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

Base Information

Chemical Name:2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine
CAS No.:1452824-45-1
Molecular Formula:C₂₄H₃₁BF₂O₆Si
Molecular Weight:492.4
Hs Code.:

Synonyms:2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

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Chemical Property of 2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

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Technology Process of 2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

There total 4 articles about 2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 998-30-1
Triethoxysilane

: 1452824-42-8
2,2-difluoro-4-phenyl-6-[3-(prop-2-en-1-yloxy)phenyl]-1,3,2-(2H)-dioxaborine

: 1452824-45-1
2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In tetrahydrofuran; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1002/hc.21091

Reference yield:

: 98-86-2
acetophenone

: 1452824-45-1
2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / benzene / 8 h / Inert atmosphere; Reflux

2: dichloromethane / 1 h / 20 °C

3: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; sodium hydride; In tetrahydrofuran; dichloromethane; benzene; 1: |Claisen Condensation;
DOI:10.1002/hc.21091

Reference yield:

: 1-phenyl-3-[3-(prop-2-en-1-yl-oxy)phenyl]propane-1,3-dione

: 1452824-45-1
2,2-difluoro-4-phenyl-6-[3-(3-(triethoxysilyl)propoxy)phenyl]-1,3,2-(2H)-dioxaborine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1 h / 20 °C

2: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hc.21091