(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol

Base Information

• Chemical Name: (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol
• CAS No.: 1101254-55-0
• Molecular Formula: C₄₁H₄₅F₁₇O₂SSi
• Molecular Weight: 952.931

Synonyms:(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol

Chemical Property of (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol

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Technology Process of (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol

There total 1 articles about (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]phenyl}-2-(tert-butyldimethylsilanyloxy)-2-phenylethanone (1101254-53-8) + phenylmagnesium bromide (100-58-3) → (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol (1101254-55-0)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.tet.2008.08.110

Reference yield: 91.0%

(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol (1101254-55-0) → (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol (1101254-58-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tet.2008.08.110

upstream raw materials:

(2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]phenyl}-2-(tert-butyldimethylsilanyloxy)-2-phenylethanone

phenylmagnesium bromide

Downstream raw materials:

(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

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