(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

Base Information

Chemical Name:(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol
CAS No.:1101254-58-3
Molecular Formula:C₃₅H₃₁F₁₇O₂S
Molecular Weight:838.669
Hs Code.:

Synonyms:(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

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Chemical Property of (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

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Technology Process of (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

There total 10 articles about (1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1101254-55-0
(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-2-(tert-butyldimethylsilanyloxy)-1,2-diphenylethanol

: 1101254-58-3
(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2008.08.110

Reference yield: 75.0%

: C₃₉H₃₅F₁₇O₃S

: 78-84-2
isobutyraldehyde

: 1101254-58-3
(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

: (4R,5R)-5-isopropyl-4-methyl-dihydrofuran-2(3H)-one

Guidance literature:: With samarium diiodide; In tert-butyl alcohol; at -15 ℃; for 5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1016/j.tet.2008.08.110

Reference yield: 70.0%

: 1101254-68-5
C₃₈H₃₃F₁₇O₃S

: 98-86-2
acetophenone

: 1101254-58-3
(1S,2R)-1-{4-[5-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)pentyl]-phenyl}-1,2-diphenylethane-1,2-diol

: 7210-42-6
(5S)-5-methyl-5-phenyldihydrofuran-2(3H)-one

: 88314-79-8
(R)-5-methyl-5-phenyl-3,4-dihydro(5H)-furan-2-one

Guidance literature:: With samarium diiodide; In tert-butyl alcohol; at -15 ℃; for 5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1016/j.tet.2008.08.110