ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

Base Information

Chemical Name:ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate
CAS No.:1056555-28-2
Molecular Formula:C₄₅H₅₈Cl₂N₂O₉
Molecular Weight:841.87
Hs Code.:

ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

Synonyms:ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

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Chemical Property of ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

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Technology Process of ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

There total 16 articles about ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056555-21-5
tert-butyl (3-[[3-hydroxy-5-(3-methoxypropyl)benzyl](cyclopropyl)amino]-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-3-oxopropyl)carbamate

: 15224-11-0
trans-ethyl 2-hydroxymethyl-1-cyclopropanecarboxylate

: 1056555-28-2
ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In toluene; at 80 ℃; for 24h;

Reference yield:

: 1026786-84-4
3-hydroxy-5-[(1E)-3-(methyloxy)-1-propen-1-yl]benzaldehyde

: 1056555-28-2
ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: magnesium sulfate / dichloromethane / 12 h / 20 °C

2.2: 3 h / 0 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 20 °C

6.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 24 h / 80 °C

With 1H-imidazole; tributylphosphine; tetrabutyl ammonium fluoride; hydrogen; magnesium sulfate; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1026786-87-7
3-((tert-butyl(dimethyl)silyl)oxy)-5-[(1E)-3-methoxy-prop-1-en-1-yl]-benzaldehyde

: 1056555-28-2
ethyl 2-(((3-(((3-(tert-butoxycarbonyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)propanoyl)(cyclopropyl)amino)methyl)-5-(3-methoxypropyl)phenoxy)methyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium sulfate / dichloromethane / 12 h / 20 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 20 °C

5.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 24 h / 80 °C

With tributylphosphine; tetrabutyl ammonium fluoride; hydrogen; magnesium sulfate; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;