cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

Base Information

Chemical Name:cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one
CAS No.:1409956-67-7
Molecular Formula:C₂₂H₂₃ClO
Molecular Weight:338.877
Hs Code.:

Synonyms:cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

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Chemical Property of cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

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Technology Process of cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

There total 10 articles about cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1409956-62-2
2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one

: 1409956-67-7
cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: With hydrogen; platinum(IV) oxide; In acetone; at 20 ℃; under 3677.86 Torr;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1409956-67-7
cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 7 steps

1.1: magnesium / iodine / tetrahydrofuran / 50 °C / Inert atmosphere

1.2: 1 h / 40 - 50 °C

2.1: toluene-4-sulfonic acid / toluene; ethylene glycol / 6 h / 110 °C

3.1: hydrogen / 3% Pd/C / ethyl acetate / 7 h / 20 °C / 3677.86 - 5149.01 Torr

4.1: toluene-4-sulfonic acid / water; acetone / 3 h / 70 °C

5.1: titanium tetrachloride / dichloromethane / -35 - 0 °C / Inert atmosphere

5.2: 1 h / -55 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / toluene / 2 h / 60 °C

7.1: hydrogen / platinum(IV) oxide / acetone / 20 °C / 3677.86 Torr

With hydrogen; titanium tetrachloride; toluene-4-sulfonic acid; magnesium; platinum(IV) oxide; 3% Pd/C; iodine; In tetrahydrofuran; dichloromethane; water; ethylene glycol; ethyl acetate; acetone; toluene; 5.1: Mukaiyama aldol condensation / 5.2: Mukaiyama aldol condensation;

Reference yield:

: 38858-72-9
1-trimethylsiloxy-3,4-dihydronaphthalene

: 1409956-67-7
cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: titanium tetrachloride / dichloromethane / -35 - 0 °C / Inert atmosphere

1.2: 1 h / -55 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 2 h / 60 °C

3.1: hydrogen / platinum(IV) oxide / acetone / 20 °C / 3677.86 Torr

With hydrogen; titanium tetrachloride; toluene-4-sulfonic acid; platinum(IV) oxide; In dichloromethane; acetone; toluene; 1.1: Mukaiyama aldol condensation / 1.2: Mukaiyama aldol condensation;