2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one

Base Information

• Chemical Name: 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one
• CAS No.: 1409956-62-2
• Molecular Formula: C₂₂H₂₁ClO
• Molecular Weight: 336.861

Synonyms:2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one

Chemical Property of 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one

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Technology Process of 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one

There total 13 articles about 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(4-chlorophenyl)-1-(1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl)cyclohexyl 2,2,2-trifluoroacetate (1421369-93-8) → 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one (1409956-62-2)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; for 5h; Reagent/catalyst; Solvent; Time; Reflux;

Reference yield: 56.0%

trans-2-(4-(4-chlorophenyl)-1-hydroxycyclohexyl)-3,4-dihydronaphthalen-1(2H)-one → 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one (1409956-62-2)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 60 ℃; for 2h;

Reference yield: 50.0%

2-(4-(4-chlorophenyl)-1-hydroxycyclohexyl)-3,4-dihydronaphthalen-1(2H)-one (1409956-58-6) → 4-(4-chlorophenyl)cyclohexan-1-one (14472-80-1) + 2-(4-(4-chlorophenyl)cyclohex-1-en-1-yl)-3,4-dihydronaphthalen-1(2H)-one (1409956-62-2) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 60 ℃; for 6h;

upstream raw materials:

cyclohexanedione monoethylene ketal

1-trimethylsiloxy-3,4-dihydronaphthalene

3,4-dihydronaphthalene-1(2H)-one

4-(4-chlorophenyl)cyclohexan-1-one

Downstream raw materials:

cis/trans-(4-(4-chlorophenyl)cyclohexyl)naphthalen-1,4-dione

trans-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

cis-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

cis/trans-2-bromo-2-(4-(4-chlorophenyl)cyclohexyl)-3,4-dihydronaphthalen-1(2H)-one

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