1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime

Base Information

• Chemical Name: 1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime
• CAS No.: 94243-20-6
• Molecular Formula: C₁₁H₁₀N₄O
• Molecular Weight: 214.227

Synonyms:1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime

Chemical Property of 1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime

Chemical Property:

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Technology Process of 1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime

There total 1 articles about 1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

Nitroethane (79-24-3) + 3-phenyl-1,2,4-triazine (24108-40-5) → 1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime (94243-20-6)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide;

DOI:10.1016/S0040-4039(01)81522-7

Reference yield: 83.0%

1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime (94243-20-6) → 1-(3-phenyl-1,2,4-triazin-5-yl)ethan-1-one (94243-24-0)

Guidance literature:

With ammonium chlorochromate on aluminum oxide; In chloroform; at 20 ℃; for 24h;

DOI:10.1080/00304940109356617

Reference yield:

1-(3-phenyl-1,2,4-triazin-5-yl)ethanone oxime (94243-20-6) → C18H17N5 (310888-36-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dithionite

2: Acidic conditions

With sodium dithionite;

upstream raw materials:

Nitroethane

3-phenyl-1,2,4-triazine

Downstream raw materials:

1-(3-phenyl-1,2,4-triazin-5-yl)ethan-1-one

C₁₈H₁₇N₅

C₁₈H₁₇N₅

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