2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

Base Information

Chemical Name:2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide
CAS No.:117293-73-9
Molecular Formula:C₁₇H₇F₁₇N₂O
Molecular Weight:578.228
Hs Code.:

Synonyms:2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

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Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

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Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

There total 4 articles about 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3544-25-0
p-aminophenylacetonitrile

: 375-95-1
perfluorononanoic acid

: 117293-73-9
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

Guidance literature:: With 1-ethoxyacetylene; In ethyl acetate; at 85 ℃; for 15h;
DOI:10.1021/jm00121a003

Reference yield:

: 3544-25-0
p-aminophenylacetonitrile

: 52447-23-1
heptadecafluorononanic acid chloride

: 117293-73-9
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jm00121a003

Reference yield:

: 375-95-1
perfluorononanoic acid

: 117293-73-9
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-N-<(4-cyanomethyl)phenyl>nonanamide

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 15 h / 85 °C

2: ethyl acetate / 24 h / Ambient temperature

In ethyl acetate;
DOI:10.1021/jm00083a021