Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)

Base Information

• Chemical Name: Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)
• CAS No.: 112220-44-7
• Molecular Formula: CF₃O₃S*C₄₄H₃₉F₃O₅P₃RuS
• Molecular Weight: 1079.91

Synonyms:Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)

Chemical Property of Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)

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Technology Process of Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)

There total 1 articles about Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={Ru(CF₃SO₃)(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[bis(dimethylsulfoxide-O)(triphos)aquaruthenium(II)] triflate (112220-39-0) → Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)(1+)*CF3SO3(1-)={Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)}(CF3SO3) (112220-44-7) + dimethyl sulfoxide (67-68-5,8070-53-9)

Guidance literature:

With CO; In dichloromethane; byproducts: H2O; stirring of soln. under CO atmosphere (15 min); pptn. (Et2O addn.), washing (Et2O), drying; elem. anal.;

Reference yield:

Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)(1+)*CF3SO3(1-)={Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)}(CF3SO3) (112220-44-7) + (C2H5)4N(1+)*Cl(1-)*2H2O=((C2H5)4N)Cl*2H2O → dichlorocarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium (37843-35-9) + tetraethylammonium trifluoromethanesulphonate (35895-69-3)

Guidance literature:

In dichloromethane; byproducts: CO; Ar atmosphere, 2 equiv. Et4NCl, stirring (30 min); evapn., recrystn. (acetone);

Reference yield:

Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)(1+)*CF3SO3(1-)={Ru(CF3SO3)(CO)2(CH3C(CH2P(C6H5)2)3)}(CF3SO3) (112220-44-7) + (C2H5)4N(1+)*Cl(1-)*2H2O=((C2H5)4N)Cl*2H2O → RuCl(CO)2(CH3C(CH2P(C6H5)2)3)(1+)*CF3SO3(1-)={RuCl(CO)2(CH3C(CH2P(C6H5)2)3)}(CF3SO3) (112220-47-0) + tetraethylammonium trifluoromethanesulphonate (35895-69-3)

Guidance literature:

In dichloromethane; Ar atmosphere, stirring (30 min); evapn., recrystn. (acetone);

upstream raw materials:

[bis(dimethylsulfoxide-O)(triphos)aquaruthenium(II)] triflate

Downstream raw materials:

dichlorocarbonyl{1,1,1-tris((diphenylphosphino)methyl)ethane}ruthenium

tetraethylammonium trifluoromethanesulphonate

RuCl(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*CF₃SO₃^(1-)={RuCl(CO)2(CH₃C(CH₂P(C₆H₅)2)3)}(CF₃SO₃)

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