3,5-diiodo-2-tosyloxybenzaldehyde

Base Information

Chemical Name:3,5-diiodo-2-tosyloxybenzaldehyde
CAS No.:904324-23-8
Molecular Formula:C₁₄H₁₀I₂O₄S
Molecular Weight:528.106
Hs Code.:

Synonyms:3,5-diiodo-2-tosyloxybenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-diiodo-2-tosyloxybenzaldehyde

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Technology Process of 3,5-diiodo-2-tosyloxybenzaldehyde

There total 1 articles about 3,5-diiodo-2-tosyloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2631-77-8
3,5-diodosalicylaldehyde

: 98-59-9
p-toluenesulfonyl chloride

: 904324-23-8
3,5-diiodo-2-tosyloxybenzaldehyde

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/b604259g

Reference yield: 94.0%

: 904324-23-8
3,5-diiodo-2-tosyloxybenzaldehyde

: 106-95-6
allyl bromide

: 3-allyl-5-iodo-2-tosyloxybenzaldehyde

Guidance literature:: 3,5-diiodo-2-tosyloxybenzaldehyde; With lithium dineopentylcuprate; In tetrahydrofuran; methanol; diethyl ether; at -78 ℃; for 0.333333h;

allyl bromide; In tetrahydrofuran; methanol; diethyl ether; at 20 ℃; Further stages.;
DOI:10.1039/b604259g

Reference yield: 80.0%

: 904324-23-8
3,5-diiodo-2-tosyloxybenzaldehyde

: 98-88-4
benzoyl chloride

: 3-benzoyl-5-iodo-2-tosyloxybenzaldehyde

Guidance literature:: 3,5-diiodo-2-tosyloxybenzaldehyde; With lithium dineopentylcuprate; In tetrahydrofuran; methanol; diethyl ether; at -78 ℃; for 0.333333h;

benzoyl chloride; In tetrahydrofuran; methanol; diethyl ether; at 20 ℃; Further stages.;
DOI:10.1039/b604259g