2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt

Base Information

• Chemical Name: 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt
• CAS No.: 1003849-06-6
• Molecular Formula: C₉H₈ClN₂OS₂*K
• Molecular Weight: 298.859
• Mol file: 1003849-06-6.mol

Synonyms:2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt

Chemical Property of 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt

There total 3 articles about 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 4-chloro-2-methylbenzohydrazide (75319-02-7) → 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt (1003849-06-6)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 5h;

DOI:10.1002/ardp.201300202

Reference yield:

4-chloro-2-methylbenzoic acid methyl ester (99585-12-3) → 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt (1003849-06-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 8 h / Reflux

2: potassium hydroxide / ethanol / 5 h / 20 °C

With hydrazine hydrate; potassium hydroxide; In ethanol;

DOI:10.1002/ardp.201300202

Reference yield:

4-chloro-2-methylbenzoic acid (7499-07-2) → 2-(4-chloro-2-methylbenzoyl)hydrazinecarbodithioic acid potassium salt (1003849-06-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / Reflux; Inert atmosphere

2: hydrazine hydrate / ethanol / 8 h / Reflux

3: potassium hydroxide / ethanol / 5 h / 20 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;

DOI:10.1002/ardp.201300202

upstream raw materials:

4-chloro-2-methylbenzoic acid methyl ester

4-chloro-2-methylbenzoic acid

carbon disulfide

4-chloro-2-methylbenzohydrazide

Downstream raw materials:

4-amino-5-(4-chloro-2-methylphenyl)-4H-1,2,4-triazole-3-thiol