N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

Base Information

Chemical Name:N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide
CAS No.:1201842-62-7
Molecular Formula:C₂₁H₁₇ClN₄O₃S
Molecular Weight:440.91
Hs Code.:

Synonyms:N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

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Chemical Property of N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

Chemical Property:

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Technology Process of N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

There total 4 articles about N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1112983-23-9
N-(2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-3-yl)-4-methoxybenzenesulfonamide

: 791626-58-9
2-amino-6-bromoquinoline

: 1201842-62-7
N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; at 90 ℃; for 2h;

Reference yield:

: 588729-99-1
3-amino-5-bromo-2-chloropyridine

: 1201842-62-7
N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 4 h / 90 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 2 h / 90 °C

With potassium acetate; sodium carbonate; lithium hexamethyldisilazane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; ethanol;

Reference yield:

: 1112982-81-6
N-(5-bromo-2-chloropyridin-3-yl)-4-methoxybenzenesulfonamide

: 1201842-62-7
N-(5-(2-amino-6-quinolinyl)-2-chloro-3-pyridinyl)-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 4 h / 90 °C / Inert atmosphere

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 2 h / 90 °C

With potassium acetate; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol;