1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

Base Information

Chemical Name:1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea
CAS No.:124794-72-5
Molecular Formula:C₂₁H₂₈N₄OS
Molecular Weight:384.546
Hs Code.:

Synonyms:1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

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Technology Process of 1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

There total 7 articles about 1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 111783-01-8
4-isothiocyanato-1-(2-(4-methoxyphenyl)ethyl)piperidine

: 95-54-5
1,2-diamino-benzene

: 124794-72-5
1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

Guidance literature:: In ethanol; ethyl acetate; at 20 ℃; for 24h;
DOI:10.1002/cmdc.201300172

Reference yield:

: 1-{1-[2-(4-Methoxy-phenyl)-ethyl]-piperidin-4-yl}-3-(2-nitro-phenyl)-thiourea

: 124794-72-5
1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

Guidance literature:: With ammonia; hydrogen; palladium on activated charcoal; In methanol; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00150a029

Reference yield:

: 85098-70-0
4-amino-1-(2-(4-methoxyphenyl)ethyl)piperidine

: 124794-72-5
1-(2-aminophenyl)-3-(1-(2-(4-methoxyphenyl)ethyl)piperidin-4-yl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 25 °C

2: H₂, NH₃ / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

With ammonia; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00150a029