[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

Base Information

Chemical Name:[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄
CAS No.:494831-50-4
Molecular Formula:C₄₈H₅₄NO₆P₂Pd*ClO₄
Molecular Weight:1008.78
Hs Code.:

[Pd(2,3-(MeO)2C<sub>6</sub>H<sub>2</sub>CH=N(Cy)-C<sub>6</sub>,N)((Ph<sub>2</sub>P)2CHCH<sub>2</sub>CH(COOEt)(COOEt)-P,P')]ClO<sub>4</sub>

Synonyms:[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

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Chemical Property of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

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Technology Process of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

There total 3 articles about [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 494831-11-7
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CCH₂-P,P')]ClO₄

: 105-53-3
diethyl malonate

: 494831-50-4
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

Guidance literature:: sodium carbonate; In chloroform; under Ar, 2 equiv. of the ester, heating in dry CHCl3 at 45 °C for 15 h in the presence of anhyd. Na2CO3; soln. was cooled to room temp., filtered through Celite, evapd. in vac.,residue was triturated with Et2O, filtered off, washed with cold Et2O, dried in vac.;
DOI:10.1039/b203864a

Reference yield:

: 494831-06-0
[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)(μ-Cl)]2

: 494831-50-4
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetone

2: sodium carbonate / chloroform

sodium carbonate; In chloroform; water; acetone;
DOI:10.1039/b203864a

Reference yield:

: 84494-89-3
1,1-bis-(diphenylphosphino)ethene

: 494831-50-4
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOEt)(COOEt)-P,P')]ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetone

2: sodium carbonate / chloroform

sodium carbonate; In chloroform; water; acetone;
DOI:10.1039/b203864a