(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

Base Information

Chemical Name:(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide
CAS No.:1331746-03-2
Molecular Formula:C₁₃H₁₂N₄O₃S
Molecular Weight:304.329
Hs Code.:

Synonyms:(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

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Technology Process of (E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

There total 1 articles about (E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18612-28-7
3-hydrazinyl-oxo-N-(1,3-thiazole-2-yl)-propanamide

: 90-02-8
salicylaldehyde

: 1331746-03-2
(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.molstruc.2011.06.050

Reference yield: 82.0%

: 1331746-03-2
(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

: 6046-93-1
copper(II) acetate monohydrate

: acetato(3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide(-1H))copper(II)

Guidance literature:: In ethanol; ligand mixed with soln. of CuCl2 in abs. EtOH; heated under reflux (water bath) for 2 h; isolated compd. washed with H2O, EtOH and Et2O; dried in desiccator overanhyd. CaCl2; elem. anal.;
DOI:10.1016/j.molstruc.2011.06.050

Reference yield: 78.0%

: copper(ll) sulfate pentahydrate

: 1331746-03-2
(E)-3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide

: 7732-18-5
water

: diaquabis(3-(2-(2-hydroxybenzylidene)hydrazinyl)-3-oxo-n(thiazole-2-yl)propanamide(-1H))copper(II)

Guidance literature:: In water; ligand mixed with soln. of CuCl2 in distd. H2O; heated under reflux (water bath) for 1 h; isolated compd. washed with H2O, EtOH and Et2O; dried in desiccator overanhyd. CaCl2; elem. anal.;
DOI:10.1016/j.molstruc.2011.06.050