allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

Base Information

• Chemical Name: allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside
• CAS No.: 583043-07-6
• Molecular Formula: C₆₄H₅₄O₁₈
• Molecular Weight: 1111.12

Synonyms:allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

Chemical Property of allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

There total 1 articles about allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate (183901-63-5) + allyl-3,4,6-tri-O-benzoyl-α-D-mannopyranoside (578007-57-5) → allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside (583043-07-6)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/S0957-4166(03)00216-7

Reference yield: 68.0%

tiolacetic acid (507-09-5) + allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside (583043-07-6) → 3-thioacetoxypropyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside (1197987-93-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In 1,4-dioxane; at 80 ℃; for 2h;

DOI:10.1002/anie.200903328

Reference yield:

allyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside (583043-07-6) → C61H50O18

Guidance literature:

With palladium dichloride; In methanol; at 20 ℃; for 4h;

DOI:10.1016/S0957-4166(03)00216-7

upstream raw materials:

2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

allyl-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

Downstream raw materials:

2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

3-thioacetoxypropyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

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