3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

Base Information

Chemical Name:3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide
CAS No.:93235-92-8
Molecular Formula:C₂₁H₂₅N₃O₅S₂*HI
Molecular Weight:591.491
Hs Code.:

Synonyms:3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

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Chemical Property of 3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

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Technology Process of 3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

There total 4 articles about 3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 93235-90-6
3-(4-Thiocarbamoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid

: 74-88-4
methyl iodide

: 93235-92-8
3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

Guidance literature:: In acetone; for 72h; Ambient temperature;

Reference yield:

: 42908-33-8
3-{[(4-methylphenyl)sulfonyl]amino}propanoic acid

: 93235-92-8
3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 1 h / Heating

2: 40 percent / NaOH (1 mol/l) / diethyl ether; H₂O / 6 h / Ambient temperature

3: 80 percent / TEA, H₂S / pyridine / 48 h / Ambient temperature

4: 75 percent / acetone / 72 h / Ambient temperature

With sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; In pyridine; diethyl ether; water; acetone;

Reference yield:

: 61341-03-5
N-(toluene-4-sulfonyl)-β-alanyl chloride

: 93235-92-8
3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-[3-(toluene-4-sulfonylamino)-propionylamino]-propionic acid; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / NaOH (1 mol/l) / diethyl ether; H₂O / 6 h / Ambient temperature

2: 80 percent / TEA, H₂S / pyridine / 48 h / Ambient temperature

3: 75 percent / acetone / 72 h / Ambient temperature

With sodium hydroxide; TEA; hydrogen sulfide; In pyridine; diethyl ether; water; acetone;