(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

Base Information

Chemical Name:(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol
CAS No.:1202520-82-8
Molecular Formula:C₄₂H₇₂O₄Si₂
Molecular Weight:697.202
Hs Code.:

(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

Synonyms:(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

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Chemical Property of (5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

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Technology Process of (5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

There total 1 articles about (5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₆₄O₄Si₂

: 927-77-5
n-propylmagnesium bromide

: 1202520-82-8
(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

Guidance literature:: C₃₉H₆₄O₄Si₂; n-propylmagnesium bromide; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; optical yield given as %de;
DOI:10.1021/ol902414u

Reference yield: 88.0%

: 1202520-82-8
(5R,6R,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-ol

: 1202520-70-4
(5S,6S,7R)-6-(tert-butyldimethylsilyloxy)-7-((2R,3S,5S,6R)-6-((S)-1-(tert-butyldiphenylsilyloxy)butan-2-yl)-3,5-dimethyltetrahydro-2H-pyran-2-yl)-5-methyloctan-4-one

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol902414u