1-phenethylcycloheptene

Base Information

Chemical Name:1-phenethylcycloheptene
CAS No.:130220-20-1
Molecular Formula:C₁₅H₂₀
Molecular Weight:200.324
Hs Code.:

Synonyms:1-phenethylcycloheptene

Suppliers and Price of 1-phenethylcycloheptene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenethylcycloheptene

Chemical Property:

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Technology Process of 1-phenethylcycloheptene

There total 8 articles about 1-phenethylcycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 130220-19-8
2-phenethyl-2-(phenylsulfonyl)-1-thiacyclooctane S,S-dioxide

: 130220-20-1
1-phenethylcycloheptene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 0.0833333h;

Reference yield:

: 17494-61-0
((3-phenylpropyl)sulfonyl)benzene

: 130220-20-1
1-phenethylcycloheptene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

2: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

3: 88 percent / acetone; H₂O / 20 h / Ambient temperature

4: tetra-n-butylammonium fluoride ((TBA)F), 4-Angstroem molecular sieves / tetrahydrofuran / -78 - 25 °C

5: ruthenium trichloride trihydrate, sodium periodate / H₂O; acetonitrile; CCl₄ / 0 - 25 °C

6: 87 percent / t-BuOK / tetrahydrofuran / 0.08 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; ruthenium trichloride; sodium periodate; n-butyllithium; 4 A molecular sieve; potassium tert-butylate; tetrabutyl ammonium fluoride; In tetrahydrofuran; tetrachloromethane; water; acetone; acetonitrile;

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 130220-20-1
1-phenethylcycloheptene

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydride / tetrahydrofuran / 1 h / 25 °C

2: 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 25 °C

3: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

4: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

5: 88 percent / acetone; H₂O / 20 h / Ambient temperature

6: tetra-n-butylammonium fluoride ((TBA)F), 4-Angstroem molecular sieves / tetrahydrofuran / -78 - 25 °C

7: ruthenium trichloride trihydrate, sodium periodate / H₂O; acetonitrile; CCl₄ / 0 - 25 °C

8: 87 percent / t-BuOK / tetrahydrofuran / 0.08 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; ruthenium trichloride; sodium periodate; n-butyllithium; 4 A molecular sieve; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; acetone; acetonitrile;