PHENYL 3-PHENYLPROPYL SULPHIDE

Base Information

• Chemical Name: PHENYL 3-PHENYLPROPYL SULPHIDE
• CAS No.: 30134-12-4
• Molecular Formula: C15H16 S
• Molecular Weight: 228.358
• Hs Code.: 2930909090
• Mol file: 30134-12-4.mol

Synonyms:1-Phenyl-3-phenylthiopropane;NSC 163395; Phenyl 3-phenylpropyl sulfide; [(3-Phenylpropyl)thio]benzene

Chemical Property of PHENYL 3-PHENYLPROPYL SULPHIDE

Chemical Property:

• Vapor Pressure: 8.26E-05mmHg at 25°C
• Boiling Point: 351.6°Cat760mmHg
• Flash Point: 158.5°C
• PSA: 25.30000
• Density: 1.06g/cm³
• LogP: 4.41150

Purity/Quality:

97% ^*data from raw suppliers

Phenyl3-Phenylpropylsulphide ^*data from reagent suppliers

Safty Information:

• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PHENYL 3-PHENYLPROPYL SULPHIDE

There total 40 articles about PHENYL 3-PHENYLPROPYL SULPHIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-Phenyl-1-propanol (122-97-4) + diphenyldisulfane (882-33-7) → phenyl 3-phenylpropyl sulfide (30134-12-4)

Guidance literature:

With tributylphosphine; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1055/s-2004-837289

Reference yield: 97.0%

methyl-phenyl-thioether (100-68-5) + 1-iodo-3-phenylpropan (4119-41-9) → phenyl 3-phenylpropyl sulfide (30134-12-4)

Guidance literature:

With N,N-dimethyl acetamide; at 160 ℃; for 6h; Schlenk technique;

DOI:10.1002/asia.201801679

Reference yield: 94.0%

1-Bromo-3-phenylpropane (637-59-2) + thiophenol (108-98-5) → phenyl 3-phenylpropyl sulfide (30134-12-4)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃;

DOI:10.1021/acs.joc.1c00292

upstream raw materials:

allylbenzene

thiophenol

1-Bromo-3-phenylpropane

1-phenyl-3-(4-trimethylsilylphenyl)thiopropane

Downstream raw materials:

trimethyl(3-phenylpropyl)silane

((3-phenylpropyl)sulfonyl)benzene

C₁₅H₁₅ClS

C₁₅H₁₄Cl₂S

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