1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

Base Information

Chemical Name:1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane
CAS No.:1396365-57-3
Molecular Formula:C₂₀H₂₅ClO₆
Molecular Weight:396.868
Hs Code.:

Synonyms:1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

Suppliers and Price of 1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

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Technology Process of 1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

There total 2 articles about 1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1396365-54-0
1-hydroxy-15-(2-hydroxyphenyl)-4,5-dibenzo-3,6,9,12,15-pentaoxapentadecane

: 1396365-57-3
1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

Guidance literature:: With pyridine; thionyl chloride; In benzene; at 80 ℃; for 8h; Inert atmosphere;
DOI:10.1002/cjoc.201100596

Reference yield:

: 68822-97-9
1,8-bis(2-hydroxyphenoxy)-3,6-dioxaoctane

: 1396365-57-3
1-chloro-15-(2-hydroxyphenyl)-4,5-dibenzo-3,9,12,15-pentaoxapentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tert-butyl alcohol / 24 h / Reflux; Inert atmosphere

2: pyridine; thionyl chloride / benzene / 8 h / 80 °C / Inert atmosphere

With pyridine; thionyl chloride; sodium hydroxide; In tert-butyl alcohol; benzene;
DOI:10.1002/cjoc.201100596